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Corrosion Mechanisms and Mechanical Behavior of Additively Manufactured 7050-Based High Strength Aluminum Alloy
Corrosion Mechanisms and Mechanical Behavior of Additively Manufactured 7050-Based High St...
Corrosion Mechanisms and Mechanical Behavior of Additively Manufactured 7050-Based High Strength Aluminum Alloy

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자료유형  
 학위논문 서양
최종처리일시  
20260209102911
ISBN  
9798263395698
DDC  
000
저자명  
Rajendran, Rupesh.
서명/저자  
Corrosion Mechanisms and Mechanical Behavior of Additively Manufactured 7050-Based High Strength Aluminum Alloy
발행사항  
[Sl] : Georgia Institute of Technology, 2023
발행사항  
Ann Arbor : ProQuest Dissertations & Theses, 2023
형태사항  
193 p
주기사항  
Source: Dissertations Abstracts International, Volume: 87-05, Section: B.
주기사항  
Advisor: Singh, Preet M.
학위논문주기  
Thesis (Ph.D.)--Georgia Institute of Technology, 2023.
초록/해제  
요약Metal additive manufacturing (AM), particularly Laser Powder Bed Fusion (L-PBF) process enables creation of complex parts with high design freedom, reduced material wastage, and improved performance; challenges that are difficult to overcome using traditional manufacturing processes. High strength aluminum alloys such as AA 7000 series offer superior strength to weight ratio, excellent corrosion resistance, and fatigue properties, making them attractive for applications within the aerospace, defense, and automotive sectors. Nonetheless, the adoption of high-strength aluminum alloys in the realm of additive manufacturing has faced notable constraints. This is attributed to the solidification and hot tearing defects formed during the AM process stemming from their columnar microstructure. Recent advancements in the inoculation process by addition of nanoparticles/in-situ reactive constituents have demonstrated their ability to promote equiaxed grain growth in high-strength aluminum alloys, effectively mitigating the defects and enhancing their printability. The rapid solidification rates of L-PBF process along with the presence of inoculating particles and alloy constituents leads to complex microstructures, much different from the traditional wrought alloys. Consequently, there is lack of an in-depth understanding regarding the material behavior of high-strength aluminum alloys fabricated via AM process with the incorporation of inoculants. Moreover, the post-processing treatments required to attain the desired microstructure for improved corrosion resistance and mechanical properties require optimization.The objective of this research work is two-fold. First, to understand the postprocessing effects of an inoculated L-PBF 7050-based high strength aluminum alloy on the microstructure and its evolution. Second, to understand the microstructural effects on three important properties from an application point of view - corrosion, stress corrosion cracking (SCC) resistance, and mechanical behavior of the alloy. The as printed material is subjected to stress relieving, hot isostatic pressing, and a combination of solutionizing and aging heat treatments. Multi-scale microstructural characterization using SEM, EBSD, and TEM/STEM is utilized to understand the grain size distribution, identify the constituent particles, including their sizes and distribution. Corrosion and SCC behavior of the AM 7050-based alloy subjected to post-processing is investigated using scanning vibrating electrode technique, cyclic polarization, electrochemical impedance spectroscopy, and slow strain rate tests. Mechanical behavior is studied using uniaxial tensile tests and hardness measurements. The results are compared to a commercial grade wrought AA 7050 alloy to understand the key differences. The results show that the size, nature, and distribution of the constituent particles is unique for the AM 7050-based alloy, and it highly depends on the post-processing route. The inoculant addition results in formation of composite like microstructure with ceramic and intermetallic particles distributed throughout a microscopic to nanoscopic scale. Overall, the AM 7050-based alloy showed enhanced corrosion resistance and mechanical properties that were comparable to those of an equivalent 7050 wrought alloy. This research work provides insights for post-processing optimization and demonstrates the potential of inoculation based AM 7050-based high strength alloys as promising candidate for future aerospace applications.
일반주제명  
Electrodes
일반주제명  
Solidification
일반주제명  
Grain boundaries
일반주제명  
Grain size
일반주제명  
Frequency distribution
일반주제명  
Microstructure
일반주제명  
Corrosion tests
일반주제명  
Stress corrosion cracking
일반주제명  
Chloride
일반주제명  
Solid solutions
일반주제명  
Grain growth
일반주제명  
Corrosion resistance
일반주제명  
Metal fatigue
일반주제명  
Ductility
일반주제명  
Aluminum alloys
일반주제명  
Fractures
일반주제명  
Particle size
일반주제명  
Corrosion potential
일반주제명  
Alloys
일반주제명  
Industrial engineering
일반주제명  
Materials science
기타저자  
Georgia Institute of Technology.
기본자료저록  
Dissertations Abstracts International. 87-05B.
전자적 위치 및 접속  
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MARC

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■00520260209102911
■006m          o    d                
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■020    ▼a9798263395698
■035    ▼a(MiAaPQ)AAI32315876
■035    ▼a(MiAaPQ)GeorgiaTech76847
■040    ▼aMiAaPQ▼cMiAaPQ
■0820  ▼a000
■1001  ▼aRajendran,  Rupesh.
■24510▼aCorrosion  Mechanisms  and  Mechanical  Behavior  of  Additively  Manufactured  7050-Based  High  Strength  Aluminum  Alloy
■260    ▼a[Sl]▼bGeorgia  Institute  of  Technology▼c2023
■260  1▼aAnn  Arbor▼bProQuest  Dissertations  &  Theses▼c2023
■300    ▼a193  p
■500    ▼aSource:  Dissertations  Abstracts  International,  Volume:  87-05,  Section:  B.
■500    ▼aAdvisor:  Singh,  Preet  M.
■5021  ▼aThesis  (Ph.D.)--Georgia  Institute  of  Technology,  2023.
■520    ▼aMetal  additive  manufacturing  (AM),  particularly  Laser  Powder  Bed  Fusion  (L-PBF)  process  enables  creation  of  complex  parts  with  high  design  freedom,  reduced  material  wastage,  and  improved  performance;  challenges  that  are  difficult  to  overcome  using  traditional  manufacturing  processes.  High  strength  aluminum  alloys  such  as  AA  7000  series  offer  superior  strength  to  weight  ratio,  excellent  corrosion  resistance,  and  fatigue  properties,  making  them  attractive  for  applications  within  the  aerospace,  defense,  and  automotive  sectors.  Nonetheless,  the  adoption  of  high-strength  aluminum  alloys  in  the  realm  of  additive  manufacturing  has  faced  notable  constraints.  This  is  attributed  to  the  solidification  and  hot  tearing  defects  formed  during  the  AM  process  stemming  from  their  columnar  microstructure.  Recent  advancements  in  the  inoculation  process  by  addition  of  nanoparticles/in-situ  reactive  constituents  have  demonstrated  their  ability  to  promote  equiaxed  grain  growth  in  high-strength  aluminum  alloys,  effectively  mitigating  the  defects  and  enhancing  their  printability.  The  rapid  solidification  rates  of  L-PBF  process  along  with  the  presence  of  inoculating  particles  and  alloy  constituents  leads  to  complex  microstructures,  much  different  from  the  traditional  wrought  alloys.  Consequently,  there  is  lack  of  an  in-depth  understanding  regarding  the  material  behavior  of  high-strength  aluminum  alloys  fabricated  via  AM  process  with  the  incorporation  of  inoculants.  Moreover,  the  post-processing  treatments  required  to  attain  the  desired  microstructure  for  improved  corrosion  resistance  and  mechanical  properties  require  optimization.The  objective  of  this  research  work  is  two-fold.  First,  to  understand  the  postprocessing  effects  of  an  inoculated  L-PBF  7050-based  high  strength  aluminum  alloy  on  the  microstructure  and  its  evolution.  Second,  to  understand  the  microstructural  effects  on  three  important  properties  from  an  application  point  of  view  -  corrosion,  stress  corrosion  cracking  (SCC)  resistance,  and  mechanical  behavior  of  the  alloy.  The  as  printed  material  is  subjected  to  stress  relieving,  hot  isostatic  pressing,  and  a  combination  of  solutionizing  and  aging  heat  treatments.  Multi-scale  microstructural  characterization  using  SEM,  EBSD,  and  TEM/STEM  is  utilized  to  understand  the  grain  size  distribution,  identify  the  constituent  particles,  including  their  sizes  and  distribution.  Corrosion  and  SCC  behavior  of  the  AM  7050-based  alloy  subjected  to  post-processing  is  investigated  using  scanning  vibrating  electrode  technique,  cyclic  polarization,  electrochemical  impedance  spectroscopy,  and  slow  strain  rate  tests.  Mechanical  behavior  is  studied  using  uniaxial  tensile  tests  and  hardness  measurements.  The  results  are  compared  to  a  commercial  grade  wrought  AA  7050  alloy  to  understand  the  key  differences.  The  results  show  that  the  size,  nature,  and  distribution  of  the  constituent  particles  is  unique  for  the  AM  7050-based  alloy,  and  it  highly  depends  on  the  post-processing  route.  The  inoculant  addition  results  in  formation  of  composite  like  microstructure  with  ceramic  and  intermetallic  particles  distributed  throughout  a  microscopic  to  nanoscopic  scale.  Overall,  the  AM  7050-based  alloy  showed  enhanced  corrosion  resistance  and  mechanical  properties  that  were  comparable  to  those  of  an  equivalent  7050  wrought  alloy.  This  research  work  provides  insights  for  post-processing  optimization  and  demonstrates  the  potential  of  inoculation  based  AM  7050-based  high  strength  alloys  as  promising  candidate  for  future  aerospace  applications.
■590    ▼aSchool  code:  0078.
■650  4▼aElectrodes
■650  4▼aSolidification
■650  4▼aGrain  boundaries
■650  4▼aGrain  size
■650  4▼aFrequency  distribution
■650  4▼aMicrostructure
■650  4▼aCorrosion  tests
■650  4▼aStress  corrosion  cracking
■650  4▼aChloride
■650  4▼aSolid  solutions
■650  4▼aGrain  growth
■650  4▼aCorrosion  resistance
■650  4▼aMetal  fatigue
■650  4▼aDuctility
■650  4▼aAluminum  alloys
■650  4▼aFractures
■650  4▼aParticle  size
■650  4▼aCorrosion  potential
■650  4▼aAlloys
■650  4▼aIndustrial  engineering
■650  4▼aMaterials  science
■690    ▼a0546
■690    ▼a0794
■71020▼aGeorgia  Institute  of  Technology.
■7730  ▼tDissertations  Abstracts  International▼g87-05B.
■790    ▼a0078
■791    ▼aPh.D.
■792    ▼a2023
■793    ▼aEnglish
■85640▼uhttp://www.riss.kr/pdu/ddodLink.do?id=T17366001▼nKERIS▼z이  자료의  원문은  한국교육학술정보원에서  제공합니다.

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