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Suppressing Intergranular Cracking in Blown Powder Laser Beam Directed Energy Deposition Additive Manufacturing of Molybdenum
Suppressing Intergranular Cracking in Blown Powder Laser Beam Directed Energy Deposition Additive Manufacturing of Molybdenum
상세정보
- 자료유형
- 학위논문 서양
- 최종처리일시
- 20260202105504
- ISBN
- 9798263325954
- DDC
- 600
- 서명/저자
- Suppressing Intergranular Cracking in Blown Powder Laser Beam Directed Energy Deposition Additive Manufacturing of Molybdenum
- 발행사항
- [Sl] : Georgia Institute of Technology, 2025
- 발행사항
- Ann Arbor : ProQuest Dissertations & Theses, 2025
- 형태사항
- 141 p
- 주기사항
- Source: Dissertations Abstracts International, Volume: 87-05, Section: B.
- 주기사항
- Advisor: Stebner, Aaron P.
- 학위논문주기
- Thesis (Ph.D.)--Georgia Institute of Technology, 2025.
- 초록/해제
- 요약Molybdenum (Mo) alloys have long been limited in their manufacturability by low room temperature ductility and oxidation concerns. Despite these issues, Mo has found valuable application in several industries requiring high temperature structural materials, such as aerospace, nuclear power, and metalworking. The geometric freedom and atmospheric control of blown powder laser beam directed energy deposition additive manufacturing (DED-LB-BP) makes it an attractive choice for expanding applications of Mo alloys.This thesis work utilizes metallurgical insight to enable DED-LB-BP of Mo by: (1) Designing a fixture to provide repeatable solidification for the comparison of alloy properties. (2) Through use of the fixture, quantitatively showing deformation twinning in molybdenum alloys with dilute rhenium additions, explaining a decades-old discussion about the efficacy of these additions as a ductilizing agent. (3) Identifying coherent thermal expansion and contraction as the cause of intergranular cracking and stochastic fluctuations in the density of pure Mo deposits, frustrating statistical determination of a processing zone where 99% density pure Mo deposits were achieved in DED-LB-BP for the first time. (4) Evaluating three different alloying approaches to reduce intergranular cracking, reduce stochastic density fluctuation, and thereby enable the development of stable, repeatable deposition of Mo-base alloys. Of the evaluated methods, grain refinement and solid solution strengthening are shown to be the most promising candidates.Altogether, this work provides valuable insight into Mo alloys themselves, as well as directions for development of new Mo alloys to reduce intergranular cracking and enable DED-LB-BP of high temperature, complex geometry components.
- 일반주제명
- Metals
- 일반주제명
- Cold
- 일반주제명
- Solidification
- 일반주제명
- Grain boundaries
- 일반주제명
- Powder metallurgy
- 일반주제명
- Copper
- 일반주제명
- Energy
- 일반주제명
- Grain size
- 일반주제명
- Aerospace engineering
- 일반주제명
- Sintering
- 일반주제명
- Annealing
- 일반주제명
- Raw materials
- 일반주제명
- Segregation
- 일반주제명
- Solid solutions
- 일반주제명
- Cooling
- 일반주제명
- Oxidation
- 일반주제명
- Carbon
- 일반주제명
- Ductility
- 일반주제명
- Extrusion dies
- 일반주제명
- Deformation
- 일반주제명
- Industrial engineering
- 일반주제명
- Materials science
- 기본자료저록
- Dissertations Abstracts International. 87-05B.
- 전자적 위치 및 접속
- 로그인 후 원문을 볼 수 있습니다.
MARC
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■00520260202105504
■006m o d
■007cr#unu||||||||
■020 ▼a9798263325954
■035 ▼a(MiAaPQ)AAI32307983
■035 ▼a(MiAaPQ)GeorgiaTech78741
■040 ▼aMiAaPQ▼cMiAaPQ
■0820 ▼a600
■1001 ▼aLies, Nathaniel Jay.
■24510▼aSuppressing Intergranular Cracking in Blown Powder Laser Beam Directed Energy Deposition Additive Manufacturing of Molybdenum
■260 ▼a[Sl]▼bGeorgia Institute of Technology▼c2025
■260 1▼aAnn Arbor▼bProQuest Dissertations & Theses▼c2025
■300 ▼a141 p
■500 ▼aSource: Dissertations Abstracts International, Volume: 87-05, Section: B.
■500 ▼aAdvisor: Stebner, Aaron P.
■5021 ▼aThesis (Ph.D.)--Georgia Institute of Technology, 2025.
■520 ▼aMolybdenum (Mo) alloys have long been limited in their manufacturability by low room temperature ductility and oxidation concerns. Despite these issues, Mo has found valuable application in several industries requiring high temperature structural materials, such as aerospace, nuclear power, and metalworking. The geometric freedom and atmospheric control of blown powder laser beam directed energy deposition additive manufacturing (DED-LB-BP) makes it an attractive choice for expanding applications of Mo alloys.This thesis work utilizes metallurgical insight to enable DED-LB-BP of Mo by: (1) Designing a fixture to provide repeatable solidification for the comparison of alloy properties. (2) Through use of the fixture, quantitatively showing deformation twinning in molybdenum alloys with dilute rhenium additions, explaining a decades-old discussion about the efficacy of these additions as a ductilizing agent. (3) Identifying coherent thermal expansion and contraction as the cause of intergranular cracking and stochastic fluctuations in the density of pure Mo deposits, frustrating statistical determination of a processing zone where 99% density pure Mo deposits were achieved in DED-LB-BP for the first time. (4) Evaluating three different alloying approaches to reduce intergranular cracking, reduce stochastic density fluctuation, and thereby enable the development of stable, repeatable deposition of Mo-base alloys. Of the evaluated methods, grain refinement and solid solution strengthening are shown to be the most promising candidates.Altogether, this work provides valuable insight into Mo alloys themselves, as well as directions for development of new Mo alloys to reduce intergranular cracking and enable DED-LB-BP of high temperature, complex geometry components.
■590 ▼aSchool code: 0078.
■650 4▼aMetals
■650 4▼aCold
■650 4▼aSolidification
■650 4▼aGrain boundaries
■650 4▼aPowder metallurgy
■650 4▼aCopper
■650 4▼aEnergy
■650 4▼aGrain size
■650 4▼aAerospace engineering
■650 4▼aSintering
■650 4▼aAnnealing
■650 4▼aRaw materials
■650 4▼aSegregation
■650 4▼aSolid solutions
■650 4▼aCooling
■650 4▼aOxidation
■650 4▼aCarbon
■650 4▼aDuctility
■650 4▼aExtrusion dies
■650 4▼aDeformation
■650 4▼aIndustrial engineering
■650 4▼aMaterials science
■690 ▼a0791
■690 ▼a0538
■690 ▼a0546
■690 ▼a0794
■71020▼aGeorgia Institute of Technology.
■7730 ▼tDissertations Abstracts International▼g87-05B.
■790 ▼a0078
■791 ▼aPh.D.
■792 ▼a2025
■793 ▼aEnglish
■85640▼uhttp://www.riss.kr/pdu/ddodLink.do?id=T17360306▼nKERIS▼z이 자료의 원문은 한국교육학술정보원에서 제공합니다.


